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Lecturer(s)
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Kalenda Petr, prof. Ing. CSc.
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Kalendová Andréa, prof. Ing. Dr.
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Veselý David, doc. Ing. Ph.D.
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Černý Michal, Ing. Ph.D.
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Course content
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Preparation of adductive polyamide curing agent for epoxy coating materials. Determination of kinetic parameters in thermally initiated styrene polymerization. Polystyrene preparation - by polymerization suspension. Phenol-formaldehyde resin (novolak) preparation - methylolation and polycondensation. Non-saturated polyester preparation, determination of kinetic parameters - polycondensation. Co-polymeric latex preparation - emulsion polymerization. Alkyd resin preparation - transesterification and polycondensation. Cellulose triacetate preparation - response to polymer, styrene desinhibition. Polyamides preparation. Polymers analysis - type qualitative determination. Viscose preparation. Polyethylenterephtalate preparation. Urea-formaldehyde resin preparation. Melaminie-formaldehyde resin preparation.
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Learning activities and teaching methods
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Laboratory work
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Learning outcomes
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Subject is conceived as a lab and serves to knowledges acquisition and practice of macromolecular chemistry, polymers preparation by polymerisation, polycondensation, polyaddition, especially polymer binding agents synthesis and some kinds of synthetic fibres synthesis. It is a follow up to the theoretical basis of subjects Polymer and composites chemistry and Film-forming agents chemistry. Aim of the subject is to acquaint the student with laboratory preparation of various kinds of polymeric materials. Another aim is improve manual skills applicable to various preparations and synthesis carried out in research laboratories.
Graduate is able to participate in works in research and development laboratories specialized for polymeric materials after the graduation from this subject.
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Prerequisites
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Basic knowledge of organic and macromolecular chemistry. Basic skill in chemical laboratory.
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Assessment methods and criteria
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Oral examination
There is an oral examination. Primary form of exam is the debate about selected themes. Level of acquired knowledge, conceptions and application acquirements is examined. Knowledge is examined by test during semester and its result is included into total classification.
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Recommended literature
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Mleziva J., Kálal J. Základy makromolekulární chemie. SNTL Praha, 1986. ISBN 04-621-86.
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Mleziva J. Výroba polymerů. VŠCHT Pardubice, 1987. ISBN 80-85113-19-8.
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Mleziva, Josef. Polymery : výroba, struktura, vlastnosti a použití. Praha: Sobotáles, 2000. ISBN 80-85920-72-7.
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