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Lecturer(s)
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Honzíček Jan, doc. Ing. Ph.D.
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Černý Michal, Ing. Ph.D.
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Podzimek Štěpán, prof. Ing. CSc.
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Machotová Jana, doc. Ing. Ph.D.
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Course content
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Week 1: Polymer structure, polymer chain models, molar mass and methods of its determination. Week 2: Viscometry of dilute polymer solutions, static and dynamic light scattering. Week 3: Chromatographic techniques with emphasis on gel permeation chromatography. Week 4: Combination of gel permeation chromatography with a light scattering detector and an online viscometer. Week 5: Asymmetric flow field flow fractionation. Week 6: Characterization of polymer branching. Week 7: Spectral methods with emphasis on infrared and Raman spectroscopy. Week 8: Magnetic resonance methods with emphasis on nuclear magnetic resonance. Week 9: Thermal methods. Week 10: Methods of mechanical evaluation. Week 11: Objective measurement of color I: Color and color of substances, visual triplet, transformation of remission curves into trichromatic values CIE XYZ, chromaticity diagrams x,y,Y, color models CIE Lab, CIE L Ch. Week 12: Objective measurement of color II: Color deviations, remission spectrophotometers, turbidity, whiteness and yellowness index, K-M equations. Week 13: Practical demonstration of instrumentation in the laboratories of the Institute of Chemistry and Technology of Macromolecular Substances and SYNPO a.s. Pardubice.
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Learning activities and teaching methods
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Monologic (reading, lecture, briefing)
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Learning outcomes
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The course introduces the basics of various analytical techniques used to characterize synthetic and natural polymers. The course also includes a practical demonstration of instrumental techniques in the laboratories of the Institute of Chemistry and Technology of Macromolecular Materials and the company SYNPO a.s. Pardubice.
The student will learn about the analysis and evaluation of various polymer materials.
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Prerequisites
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Basic knowledge of organic, analytic, and macromolecular chemistry.
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Assessment methods and criteria
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Oral examination, Written examination
Final test. Oral examination.
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Recommended literature
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Dannhoferová, Jana. Velká kniha barev : kompletní průvodce pro grafiky, fotografy a designéry. Brno: Computer Press, 2012. ISBN 978-80-251-3785-7.
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Ebner, Marc. Color constancy. Chichester: John Wiley & Sons, 2007. ISBN 978-0-470-05829-9.
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Mleziva, Josef. Polymery : výroba, struktura, vlastnosti a použití. Praha: Sobotáles, 2000. ISBN 80-85920-72-7.
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Podzimek Štěpán. Light Scattering, Size Exclusion Chromatography and Asymmetric Flow Field Flow Fractionation. 2011. ISBN 978-0-470-38617-0.
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Šňupárek, Jaromír. Makromolekulární chemie : úvod do chemie a technologie polymerů. Pardubice: Univerzita Pardubice, 2014. ISBN 978-80-7395-761-2.
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