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Lecturer(s)
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Matvieiev Oleksandr, Ph.D.
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Navrátil Michal, Ing.
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Krejčová Anna, doc. Ing. Ph.D.
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Černohorský Tomáš, doc. Ing. CSc.
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Šelešovská Renáta, doc. Ing. Ph.D.
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Course content
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Lectures, seminars 1st week: Sampling procedures, treatment and preservation of samples. 2nd week: Determination of aggregates in water in the evaluation of technological and wastewater treatment plants (pH, conductivity, neutralization capacity, COD, BOD) 3rd week: Determination of aggregates in water in the evaluation of technological and sewage plants (TOC, AOX, NEL) 4th week: Determination of metals using volumetric analysis and selected instrumental methods 5th week: Determination of metals using optical methods 6th week: Determination of non-metals and their compounds using selected instrumental methods 7th week: Determination of non-metals and their compounds using automatic analyzers 8th week: Methods of isolation of organic matter from matrix 9th week: Determination of nitro compounds, phenols, formaldehyde and other selected organic compounds 10th week: Determination of VOC, PAH, PCB, PCDD and PCDF 11th week: Evaluation and analysis of solid waste and soils 12th week: Methods of chemical analysis of sludge and sediments 13th week: Elemental analysis techniques for solid samples A Lab exercise 1st week: Introduction to the subject, introduction to principles of good laboratory practice and safety of work 2nd week: Determination of basic technological indicators of water quality - COD, water hardness, chlorides, neutralization capacity (titration) 3rd week: Determination of total dissolved and undissolved substances and total organic carbon 4th week: Determination of adsorbable organically bound halogens (AOX) 5th week: Determination of nickel content in plating bath and rinsing waters from galvanic processes (voltammetry) 6th week: Spectrophotometric determination of trivalent and hexavalent chromium content in waste water from leather processing 7th week: Qualitative evaluation and determination of pesticides in the mixture using LC-DAD/MS 8th week: Monitoring of hazardous substances according to the RoHS directive: microwave mineralization and elemental analysis using ICP OES 9th week: Voltammetric determination of selected organic compounds 10th week: Design of an experimental plan for the analysis of hazardous substances according to the ROHs Directive; screening analysis of hazardous substances in electrical equipment (XRF) 11th week: Checking the purity of organic solvents for extraction techniques using gas chromatography 12th week: Solution of practical problems of production quality control - Excursion Mangan Chvaletice, s.r.o. 13th week: Protocol consultation, replacement of non-absovated tasks
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Learning activities and teaching methods
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unspecified, Monologic (reading, lecture, briefing)
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Learning outcomes
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The aim of the course is to acquaint students with the possibility of using basic analytical methods in the field of monitoring and control of chemical technology processes.
Students will acquire knowledge and skills in the application especially of instrumental analytical methods in the field of monitoring of chemical-technological processes. They will get acquainted with specific procedures of determination of aggregate indicators in the evaluation of technological and sewage plants waters and simultaneously with procedures of determination of selected substances or groups of substances important both in terms of chemical-technological operations and in terms of possible adverse impacts of chemical production on the environment.
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Prerequisites
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Completion of courses of basic analytical chemistry and instrumental analytical chemistry in the scope of bachelor study.
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Assessment methods and criteria
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Oral examination, Written examination, Student performance assessment
Computational written exam, oral theoretical exam, active work on seminars, laboratory protocols.
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Recommended literature
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Chýlková J., a kol.: Ekoanalýza I. Pardubice: Univerzita Pardubice 2013..
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Návody k laboratorním úlohám dostupné v systému STAG. Pardubice: Univerzita Pardubice, 2018..
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Opekar F., a kol.: Základní analytická chemie. Praha: Univerzita Karlova v Praze, Karolinum, 2003..
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Seidlerová J. a kol.: Analytická chemie odpadních materiálů. Ostrava: VŠB ? Technická univerzita Ostrava, 2006..
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Skoog D. A. a kol. Principles of Instrumental Analysis. USA: Harcourt Brace & Company, 1998..
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Šelešovská R., a kol.: Ekoanalýza II. Pardubice: Univerzita Pardubice 2013..
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