| Course title | Synthhesis and Characterization of Materials - Laboratory. |
|---|---|
| Course code | UENM/C095 |
| Organizational form of instruction | Lesson |
| Level of course | Master |
| Year of study | not specified |
| Semester | Winter |
| Number of ECTS credits | 5 |
| Language of instruction | Czech |
| Status of course | Compulsory |
| Form of instruction | Face-to-face |
| Work placements | This is not an internship |
| Recommended optional programme components | None |
| Lecturer(s) |
|---|
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| Course content |
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Safety in chemical lab, safety during work with energetic materials. Chemical literature. Aromatic nitration. Thin layer chromatography (TLC), high performance liquid chromatography (HPLC), infrared spectroscopy (IR), ultraviolet spectroscopy (UV). Colour reactions in identification of energetic materials. 2,4,6-Trinitrochlorbenzene preparation and its use in the synthesis of thermally stable polynitrocompounds.
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| Learning activities and teaching methods |
| Laboratory work |
| Learning outcomes |
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To introduce safety precautions during the work with energetic materials To introduce how to work with chemical literature and to use properly present information sources. To introduce selected reactions used in the synthesis of energetic materials and their possible characterisation.
To work safely with energetic materials. To know how to find information about energetic materials in chemical literature. To choose the method of characterisation of energetic materials. |
| Prerequisites |
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C002 Laboratory of general and inorganic chemistry I C009 Laboratory of organic chemistry I
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| Assessment methods and criteria |
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Work-related product analysis
Supervision of the protocols and final report. |
| Recommended literature |
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| Study plans that include the course |
| Faculty | Study plan (Version) | Category of Branch/Specialization | Recommended semester | |
|---|---|---|---|---|
| Faculty: Faculty of Chemical Technology | Study plan (Version): Theory and Technology of Explosives (2016) | Category: Engineering chemistry and chemistry of silicates | 1 | Recommended year of study:1, Recommended semester: Winter |
| Faculty: Faculty of Chemical Technology | Study plan (Version): Theory and Technology of Explosives (2013) | Category: Engineering chemistry and chemistry of silicates | 1 | Recommended year of study:1, Recommended semester: Winter |
| Faculty: Faculty of Chemical Technology | Study plan (Version): Theory and Technology of Explosives (2015) | Category: Engineering chemistry and chemistry of silicates | 1 | Recommended year of study:1, Recommended semester: Winter |