University of Pardubice
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for academic year 2016/2017
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Course: Laboratory I

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Course title Laboratory I
Course code UENM/C097
Organizational form of instruction Lesson
Level of course Master
Year of study not specified
Semester Summer
Number of ECTS credits 10
Language of instruction Czech
Status of course unspecified
Form of instruction Face-to-face
Work placements This is not an internship
Recommended optional programme components None
Lecturer(s)
  • Pachman Jiří, doc. Ing. Ph.D.
  • Jungová Marcela, Ing. Ph.D.
  • Šelešovský Jakub, Ing. Ph.D.
  • Jalový Zdeněk, doc. Ing. Ph.D.
  • Pelikán Vojtěch, Ing. Ph.D.
  • Matyáš Robert, doc. Ing. Ph.D.
Course content
Primary nitramines. Nitrolysis of hexamethylenetetraamine. Crystallization of NTO. Determination of crystal size and shape. Esterification, esters of nitric acid. Thermal analysis. Individual literature search on the synthesis of compound, synthesis and characterization.

Learning activities and teaching methods
Laboratory work
Learning outcomes
To introduce safety precautions during the work with energetic materials. To introduce main reactions used in the synthesis of energetic materials. To introduce methods for determination of thermal stability of explosives.
Individual search of information about synthesis, selection of suitable method and safe preparation of the compound. Basic assessment of thermal stability of the substance.
Prerequisites
C893 Explosion physics I C095 Laboratory of synthesis and characterisation of materials

Assessment methods and criteria
Work-related product analysis

Supervision of the protocols and final report.
Recommended literature
  • Denkstein J. a kol. Příručka pro laboratorní cvičení v technologii zvláštních výrob, VŠCHT Pardubice, SNTL Praha (1957). SNTL Praha, 1957.
  • Fedoroff B.F., Sheffield O.E., Kaye S.M. Encyclopedia of Explosives and Related Items, Picatinny Arsenal, Dover, vol. 1-10 (1960-1983).. KTTV, Univerzita Pardubice, 2003.
  • Kalfus K., Kaválek J., Panchartek J., Socha J., Večeřa M. Organická chemie III, SNTL Praha (1978).. Picatinny Arsenal, Dover, 1983.
  • Urbanski T. Chemistry and Technology of Explosives, vol. 4, Pergamon Press, Oxford (1984).. Pergamon Press, Oxford, 1984.
  • Vymětal, J. a kol. Odborná literatura a informace v chemii, Orac, Praha (2001).. Orac, Praha, 2001.


Study plans that include the course
Faculty Study plan (Version) Category of Branch/Specialization Recommended year of study Recommended semester
Faculty: Faculty of Chemical Technology Study plan (Version): Theory and Technology of Explosives (2013) Category: Engineering chemistry and chemistry of silicates 1 Recommended year of study:1, Recommended semester: Summer
Faculty: Faculty of Chemical Technology Study plan (Version): Theory and Technology of Explosives (2016) Category: Engineering chemistry and chemistry of silicates 1 Recommended year of study:1, Recommended semester: Summer
Faculty: Faculty of Chemical Technology Study plan (Version): Theory and Technology of Explosives (2015) Category: Engineering chemistry and chemistry of silicates 1 Recommended year of study:1, Recommended semester: Summer
University of Pardubice, date of update: 11.07.2025 23:50. Data created for academic year 2016/2017