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Lecturer(s)
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Řezková Soňa, Ing. Ph.D.
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Krejčová Anna, doc. Ing. Ph.D.
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Hájek Tomáš, Ing. Ph.D.
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Fischer Jan, doc. Ing. CSc.
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Husáková Lenka, doc. Ing. Ph.D.
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Mikysek Tomáš, doc. Ing. Ph.D.
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Bajer Tomáš, doc. Ing. Ph.D.
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Česla Petr, doc. Ing. Ph.D.
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Adam Martin, doc. Ing. Ph.D.
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Metelka Radovan, Ing. Ph.D.
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Červenka Libor, doc. Ing. Ph.D.
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Course content
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1.-13. week Completion of prescribed tasks No. 1-13 (student rotation on individual tasks) Task 1 Liquid chromatography Task 2 FT-IR spectrometry Task 3 Electrochemical determination of alkaloids Task 4 Gas chromatography - ethanol and spirits Task 5 ET-AAS, microwave decompositions, trace analysis of Hg Task 6 Capillary zone electrophoresis Task 7 Isotachophoresis Task 8 Trace analysis, HPLC Task 9 UV spectrometry Task 10 Gas chromatography - profile of volatile substances, identification Task 11 Sorption isotherms, color measurement Task 12 Elemental analysis of beverages Task 13 Determination of caffeine - MEKC, UHPLC
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Learning activities and teaching methods
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Laboratory work
- Practical training
- 104 hours per semester
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Learning outcomes
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The aim of this course is to acquaint students with modern laboratory methods of inorganic and organic instrumental analysis, that may be encountered in practice. Laboratory is equipped with appropriate instrumentation for processing and analyzing of samples and computers for collecting and evaluating experimental data.
Students will be able to solve real problems in analytical laboratory equipped with modern instrumental apparatuses.
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Prerequisites
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Knowledges of analytical, physical (and organic) chemistry on the bachelor degree level.
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Assessment methods and criteria
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Written examination, Student performance assessment
Completion of all laboratory tasks - 60% of the grade Written tests always in the middle and at the end of the laboratories - 40% of the grade
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Recommended literature
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Černohorský, Tomáš . Atomová absorpční spektrometrie I : základní kurz. Praha: Spektroskopická společnost Jana Marca Marci, 2003. ISBN 80-7080-513-7.
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Jandera, Pavel. Atomová a molekulová spektroskopie se zaměřením na stopovou analýzu kontaminantů.. Pardubice: Univerzita Pardubice, 2011. ISBN 978-80-7395-392-8.
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Kolektiv autorů. Návody k jedotlivým úlohám - STAG. STAG. Pardubice, 2020.
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Kolektiv autorů. Tištěné návody k jednotlivým úlohám - k dispozici u úlohy. Pardubice, 2020.
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Lehotay, Jozef. Separačné metódy v analytickej chémii. Bratislava: Slovenská technická univerzita, 2009. ISBN 978-80-227-3036-5.
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Milata, Viktor. Vybrané metódy molekulovej spektroskopie. Bratislava: Slovenská technická univerzita, 2007. ISBN 978-80-227-2618-4.
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Nováková, Lucie. Moderní HPLC separace v teorii a praxi. Hradec Králové: Nováková Lucie, 2013. ISBN 978-80-260-4243-3.
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