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Lecturer(s)
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Kalendová Petra, Ing. Ph.D.
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Košťál Petr, Ing. Ph.D.
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Honcová Pavla, doc. Ing. Ph.D.
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Bělina Petr, Ing. Ph.D.
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Šulcová Petra, prof. Ing. Ph.D.
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Luxová Jana, Ing. Ph.D.
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Dohnalová Žaneta, doc. Ing. Ph.D.
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Course content
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OSH and FP (occupational safety and health and fire protection) at University of Pardubice and Department of Inorganic technology. Differential scanning calorimetry. Measurement of heat capacities. Crystallization from solution. Pre-treatment of material by crushing and grinding in a jet mill. Measurement of size distribution of powder materials. Colour measurement of layers. Physical properties of powder materials. Encapsulation and granulation of powder materials. Ion chromatography. Photometric determination of phosphorus. Atomic absorption spectroscopy. Final written test and total evaluation of the subject Laboratory of Synthesis and Characterization of Materials.
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Learning activities and teaching methods
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Methods of individual activities, Demonstration, Laboratory work
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Learning outcomes
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The aim of the subject is to familiarize with chosen methods for preparation and characterization of inorganic pigments, industrial fertilizers and with utilization of calorimetric methods for study of materials properties and technological processes.
Passing the subject bring to student the ability use methods for particle materials characterization (pigments, fertilizers). They are competent to decide about choice of method appropriate for obtaining of information about studied inorganic materials.
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Prerequisites
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Knowledge of courses: General and Inorganic Chemistry Laboratory, Laboratory of Analytical Instrumental Method, Chemical Engineering Laboratory Practise.
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Assessment methods and criteria
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Home assignment evaluation
The way of passing the subject is by form of classified examination. Students are monitored by laboratory practice. The laboratory reports are judged by teachers. The part of result make the written test.
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Recommended literature
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České technické normy.
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ČSN EN ISO 787-10. Všeobecné metody zkoušení pigmentů a plniv - Část 10: Stanovení hustoty - Pyknometrická metoda (vydáno1.11. 1997). 1997.
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ČSN 011718. Měření barev (vydáno 14. 5. 1990). 1990.
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Lee H.CH. Color Imaging Science, Cambridge University Press. Cambridge, 2005.
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Merkus H.G. Particle size measurements, Springer Science+Business Media B.V.. Printforce, 2009.
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Mishra M. Handsbook of Encapsulation and Controlled Release, CRC Press Taylor&Francis Group. Boca Raton, 2016.
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Moore W.J. Physical Chemistry. Prentice Hall, Inc., New Jersey, 1972.
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Šulcová P., Beneš L. Experimentální metody v anorganické technologii. Pardubice: Universita, 2008. ISBN 80-7194-420-3.
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Šulcová P., Dohnalová Ž. Anorganické pigmenty, vlastnosti a metody hodnocení. Pardubice: Universita, 2015. ISBN 978-80-7395-947-0.
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