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Lecturer(s)
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Kucek Vladimír, Ing. Ph.D.
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Dostál Libor, doc. Ing. Ph.D.
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Erben Milan, doc. Ing. Ph.D.
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Nádvorník Milan, doc. Ing. CSc.
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Vinklárek Jaromír, prof. Ing. Dr.
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Schwarz Jiří, Ing. Ph.D.
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Ruleová Pavlína, Ing. Ph.D.
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Pálka Karel, doc. Ing. Ph.D.
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Course content
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- preparation of [Ni(NH3)6]Cl2 and NiCl2 (5.4.A1) - preparation of CuCl, trans-[Cu(H2O)2(salic)2].2H2O and trans-[Cu-(salic)2] (5.4.A4a, 5.4.A4b) - preparation of K2CrO4 and K2Cr2O7, (6.3) - preparation of trans-[Co(en)2NO2]NO3 (Oh) anf Hg[Co(NCS)4](Td) (lit.(6), 5.4.A2) - preparation of SnBr4 (minidestilation) (6.14.) - preparation of Cl2 and PbO2, preparation of Pb(NO3)2 (6.5. by lit. (3), exercise 12.3.9) - electrolysis (4.1 - 4.3.) - preparation of BaCS3, (6.6) - preparation of K3[Cr(ox)3].3H2O and K3[Cr(SCN)6].4H2O (5.4.B3, 5.4.B4) - preparation of VO(acac)2, Cr(acac)3, (Inorg. Synth. 5, 113-115, 8.9.2.) - preparation of K3[Fe(CN)6] (5.4.B5) - closing exam (60 min.)
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Learning activities and teaching methods
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Laboratory work
- unspecified
- 25 hours per semester
- unspecified
- 5 hours per semester
- unspecified
- 70 hours per semester
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Learning outcomes
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Laboratory Practice of General and Inorganic Chemistry II is continuation of Laboratory Practice of General and Inorganic Chemistry I. This course aimed in learning advanced laboratory techniques and preparations.
The student will be able to prepare inorganic compounds and complexes using advanced laboratory techniques.
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Prerequisites
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Fundamental theoretical and mathematical knowledge from general and inorganic chemistry. Passing out the course Laboratory Practice of General and Inorganic Chemistry I.
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Assessment methods and criteria
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Oral examination, Written examination
During the semester the readiness of students is continuously controled using written and oral tests. Overall classification consists of experimental results, results of the continuous tests and written examination.
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Recommended literature
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Handlíř K., Mošner P., Nádvorník M., Vlček M. Laboratorní cvičení z obecné chemie..
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Handlíř K., Nádvorník M., Vlček M. Laboratorní cvičení z anorganické chemie.
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Handlíř K., Nádvorník M., Vlček M. Výpočty a cvičení z obecné a anorganické chemie I..
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Klikorka J., Klazar J., Horák J., Votinský J. Základy preparativní anorganické chemie. III. vydání, SNTL, Praha 1974..
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Nádvorník M., Handlíř K. .: Návody pro laboratorní cvičení z předmětu "Chemie organokovových sloučenin". Interní skriptum katedry obecné a anorganické chemie. 45 s. FCHT, Univerzita Pardubice 1994. Upravené vydání 2000, k disposici též na katedrálních webových stránkách..
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Rendle P., Vokins M., Davis P. Experimental Chemistry. A Laboratory Manual. Second Edition, E. Arnold Ltd., London 1972..
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