Course title | Laboratory of Synthesis and material characterization |
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Course code | UCHTML/C087 |
Organizational form of instruction | Lesson |
Level of course | Master |
Year of study | 1 |
Semester | Winter |
Number of ECTS credits | 4 |
Language of instruction | Czech |
Status of course | Compulsory |
Form of instruction | Face-to-face |
Work placements | This is not an internship |
Recommended optional programme components | None |
Lecturer(s) |
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Course content |
Preparation of adductive polyamide curing agent for epoxy coating materials. Determination of kinetic parameters in thermally initiated styrene polymerization. Polystyrene preparation - by polymerization suspension. Phenol-formaldehyde resin (novolak) preparation - methylolation and polycondensation. Non-saturated polyester preparation, determination of kinetic parameters - polycondensation. Co-polymeric latex preparation - emulsion polymerization. Alkyd resin preparation - transesterification and polycondensation. Cellulose triacetate preparation - response to polymer, styrene desinhibition. Polyamides preparation. Polymers analysis - type qualitative determination. Viscose preparation. Polyethylenterephtalate preparation. Urea-formaldehyde resin preparation. Melaminie-formaldehyde resin preparation.
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Learning activities and teaching methods |
Work with text (with textbook, with book), Laboratory work |
Learning outcomes |
Subject is conceived as a lab and serves to knowledges acquisition and practice of macromolecular chemistry, polymers preparation by polymerisation, polycondensation, polyaddition, especially polymer binding agents synthesis and some kinds of synthetic fibres synthesis. It is a follow up to the theoretical basis of subjects Polymer and composites chemistry and Film-forming agents chemistry. Aim of the subject is to acquaint the student with laboratory preparation of various kinds of polymeric materials. Another aim is improve manual skills applicable to various preparations and synthesis carried out in research laboratories.
Graduate is able to participate in works in research and development laboratories specialized for polymeric materials after the graduation from this subject. |
Prerequisites |
Basic knowledge of organic and macromolecular chemistry. Basic skill in chemical laboratory.
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Assessment methods and criteria |
Oral examination
There is an oral examination. Primary form of exam is the debate about selected themes. Level of acquired knowledge, conceptions and application acquirements is examined. Knowledge is examined by test during semester and its result is included into total classification. |
Recommended literature |
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Study plans that include the course |
Faculty | Study plan (Version) | Category of Branch/Specialization | Recommended semester | |
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Faculty: Faculty of Chemical Technology | Study plan (Version): Organic Coatings and Paints (2016) | Category: Engineering chemistry and chemistry of silicates | 1 | Recommended year of study:1, Recommended semester: Winter |
Faculty: Faculty of Chemical Technology | Study plan (Version): Technology of Polymers Manufacturing and Processing (2015) | Category: Engineering chemistry and chemistry of silicates | 1 | Recommended year of study:1, Recommended semester: Winter |
Faculty: Faculty of Chemical Technology | Study plan (Version): Fibres and Textile Chemistry (2016) | Category: Engineering chemistry and chemistry of silicates | 1 | Recommended year of study:1, Recommended semester: Winter |
Faculty: Faculty of Chemical Technology | Study plan (Version): Organic Coatings and Paints (2015) | Category: Engineering chemistry and chemistry of silicates | 1 | Recommended year of study:1, Recommended semester: Winter |
Faculty: Faculty of Chemical Technology | Study plan (Version): Fibres and Textile Chemistry (2015) | Category: Engineering chemistry and chemistry of silicates | 1 | Recommended year of study:1, Recommended semester: Winter |
Faculty: Faculty of Chemical Technology | Study plan (Version): Organic Coatings and Paints (2013) | Category: Engineering chemistry and chemistry of silicates | 1 | Recommended year of study:1, Recommended semester: Winter |
Faculty: Faculty of Chemical Technology | Study plan (Version): Technology of Polymers Manufacturing and Processing (2016) | Category: Engineering chemistry and chemistry of silicates | 1 | Recommended year of study:1, Recommended semester: Winter |