| Course title | Laboratory I |
|---|---|
| Course code | UENM/C097 |
| Organizational form of instruction | Lesson |
| Level of course | Master |
| Year of study | 1 |
| Semester | Summer |
| Number of ECTS credits | 10 |
| Language of instruction | Czech |
| Status of course | Compulsory |
| Form of instruction | Face-to-face |
| Work placements | This is not an internship |
| Recommended optional programme components | None |
| Lecturer(s) |
|---|
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| Course content |
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Primary nitramines. Nitrolysis of hexamethylenetetraamine. Crystallization of NTO. Determination of crystal size and shape. Esterification, esters of nitric acid. Thermal analysis. Individual literature search on the synthesis of compound, synthesis and characterization.
|
| Learning activities and teaching methods |
| Laboratory work |
| Learning outcomes |
|
To introduce safety precautions during the work with energetic materials. To introduce main reactions used in the synthesis of energetic materials. To introduce methods for determination of thermal stability of explosives.
Individual search of information about synthesis, selection of suitable method and safe preparation of the compound. Basic assessment of thermal stability of the substance. |
| Prerequisites |
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C893 Explosion physics I C095 Laboratory of synthesis and characterisation of materials
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| Assessment methods and criteria |
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Work-related product analysis
Supervision of the protocols and final report. |
| Recommended literature |
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| Study plans that include the course |
| Faculty | Study plan (Version) | Category of Branch/Specialization | Recommended semester | |
|---|---|---|---|---|
| Faculty: Faculty of Chemical Technology | Study plan (Version): Theory and Technology of Explosives (2013) | Category: Engineering chemistry and chemistry of silicates | 1 | Recommended year of study:1, Recommended semester: Summer |
| Faculty: Faculty of Chemical Technology | Study plan (Version): Theory and Technology of Explosives (2016) | Category: Engineering chemistry and chemistry of silicates | 1 | Recommended year of study:1, Recommended semester: Summer |
| Faculty: Faculty of Chemical Technology | Study plan (Version): Theory and Technology of Explosives (2015) | Category: Engineering chemistry and chemistry of silicates | 1 | Recommended year of study:1, Recommended semester: Summer |