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Course info
KANT / C070
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Course description
Department/Unit / Abbreviation
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KANT
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C070
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Academic Year
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2023/2024
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Academic Year
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2023/2024
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Title
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Laboratory of Synthesis and Character.
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Form of course completion
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Examination
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Form of course completion
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Examination
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Long Title
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Laboratory of Synthesis and Characterisation of Materials
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Accredited / Credits
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Yes,
7
Cred.
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Type of completion
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Combined
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Type of completion
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Combined
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Time requirements
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Laboratoř
7
[HRS/WEEK]
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Course credit prior to examination
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No
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Course credit prior to examination
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No
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Automatic acceptance of credit before examination
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No
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Included in study average
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YES
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Language of instruction
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Czech
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Occ/max
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Automatic acceptance of credit before examination
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No
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Summer semester
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0 / -
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0 / -
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0 / -
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Included in study average
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YES
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Winter semester
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1 / -
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0 / -
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0 / -
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Repeated registration
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NO
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Repeated registration
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NO
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Timetable
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Yes
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Semester taught
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Winter semester
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Semester taught
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Winter semester
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Minimum (B + C) students
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not determined
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Optional course |
Yes
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Optional course
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Yes
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Language of instruction
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Czech
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Internship duration
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0
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No. of hours of on-premise lessons |
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Evaluation scale |
A|B|C|D|E|F |
Periodicity |
každý rok
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Periodicita upřesnění |
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Fundamental theoretical course |
No
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Fundamental course |
Yes
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Fundamental theoretical course |
No
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Evaluation scale |
A|B|C|D|E|F |
Substituted course
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None
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Preclusive courses
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N/A
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Prerequisite courses
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N/A
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Informally recommended courses
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N/A
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Courses depending on this Course
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KANT/C073, KANT/C152
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Histogram of students' grades over the years:
Graphic PNG
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XLS
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Course objectives:
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The aim of the subject is to familiarize with chosen methods for preparation and characterization of inorganic pigments, industrial fertilizers and with utilization of calorimetric methods for study of materials properties and technological processes.
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Requirements on student
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The way of passing the subject is by form of classified examination. Students are monitored by laboratory practice. The laboratory reports are judged by teachers. The part of result make the written test.
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Content
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OSH and FP (occupational safety and health and fire protection) at University of Pardubice and Department of Inorganic technology.
Differential scanning calorimetry.
Measurement of heat capacities.
Crystallization from solution.
Pre-treatment of material by crushing and grinding in a jet mill.
Measurement of size distribution of powder materials.
Colour measurement of layers.
Physical properties of powder materials.
Encapsulation and granulation of powder materials.
Ion chromatography.
Photometric determination of phosphorus.
Atomic absorption spectroscopy.
Final written test and total evaluation of the subject Laboratory of Synthesis and Characterization of Materials.
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Activities
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Fields of study
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Guarantors and lecturers
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Guarantors:
Ing. Jana Luxová, Ph.D. (100%),
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Tutorial lecturer:
Ing. Petr Bělina, Ph.D. (100%),
doc. Ing. Žaneta Dohnalová, Ph.D. (100%),
doc. Ing. Pavla Honcová, Ph.D. (100%),
Ing. Petr Košťál, Ph.D. (100%),
Ing. Jana Luxová, Ph.D. (100%),
prof. Ing. Petra Šulcová, Ph.D. (100%),
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Literature
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Basic:
Šulcová P., Dohnalová Ž. Anorganické pigmenty, vlastnosti a metody hodnocení. Universita Pardubice, 2015. ISBN 978-80-7395-947-0.
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Basic:
České technické normy.
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Basic:
Šulcová P., Beneš L. Experimentální metody v anorganické technologii. Universita Pardubice, 2008. ISBN 80-7194-420-3.
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Basic:
ČSN 011718. Měření barev (vydáno 14. 5. 1990). 1990.
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Basic:
Návody pro laboratoře syntézy a charakterizace materiálů
(Bělina P., Dohnalová Ž., Drobná H., Honcová P., Kalendová P., Košťál P., Luxová J., Svoboda L., Šulcová P.)
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Basic:
ČSN EN ISO 787-10. Všeobecné metody zkoušení pigmentů a plniv - Část 10: Stanovení hustoty - Pyknometrická metoda (vydáno1.11. 1997). 1997.
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Recommended:
Lee H.CH. Color Imaging Science, Cambridge University Press. Cambridge, 2005.
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Recommended:
Mishra M. Handsbook of Encapsulation and Controlled Release, CRC Press Taylor&Francis Group. Boca Raton, 2016.
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Recommended:
Merkus H.G. Particle size measurements, Springer Science+Business Media B.V.. Printforce, 2009.
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Recommended:
Moore W.J. Physical Chemistry. Prentice Hall, Inc., New Jersey, 1972.
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Prerequisites - other information about course preconditions |
Knowledge of courses: General and Inorganic Chemistry Laboratory, Laboratory of Analytical Instrumental Method, Chemical Engineering Laboratory Practise. |
Competences acquired |
Passing the subject bring to student the ability use methods for particle materials characterization (pigments, fertilizers). They are competent to decide about choice of method appropriate for obtaining of information about studied inorganic materials. |
Teaching methods |
- Methods of individual activities
- Demonstration
- Laboratory work
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Assessment methods |
- Home assignment evaluation
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